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Simultaneous Determination of Plasticizers in Food Simulants Using GC/MS

첫 페이지 보기
  • 발행기관
    한국포장학회 바로가기
  • 간행물
    한국포장학회지 바로가기
  • 통권
    Vol. 15 No. 3 (2009.12)바로가기
  • 페이지
    pp.93-98
  • 저자
    Na Young Park, Hae Jung Yoon, In Shin Kwak, Dae Hoon Jeon, Hyun Chul Choi, Mi Ok Eum, Hyung Il Kim, Jun Hyun Sung, So Hee Kim, Young Ja Lee
  • 언어
    한국어(KOR)
  • URL
    https://www.earticle.net/Article/A277305

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원문정보

초록

영어
Migration levels of plasticizers, di-n-butyl phthalate (DBP), benzyl-butyl phthalate (BBP), di-n- octyl phthalate (DNOP), di-iso-decyl phthalate (DIDP) and di-iso-nonyl phthalate (DINP), di-(2-ethylhexyl) adipate (DEHA), from 46 poly(vinyl chloride) (PVC) wrap films and 54 PVC gaskets into food simulants were determined using gas chromatography/ mass spectrometry (GC/MS). The method was validated with limit of detection (LOD) of 0.01 ~ 0.02 μg/mL for DBP, BBP, DNOP and DEHA, and 2 μg/mL for DIDP and DINP. The linearity were found to be > 0.99 for all the compounds in concentration range of 0.1 ~ 81.4 μg/mL, and overall recoveries were ranged from 90.4 ~ 99.6%. DBP, BBP, DNOP, DEHA, DIDP and DINP were not detected in food simulants, except 1 wrap sample from which 0.28 and 0.99 μg/mL of DEHA were detected respectively when tested with 20% ethanol and n-heptane as food simulants. These values were below the regulatory limitation in European Union (EU).

목차

Abstract.
 서론
 재료 및 방법
  1. 실험재료
  2. 시약 및 시액
  3. 표준용액의 조제
  4. 시험용액의 조제
  5. 분석기기 및 방법
 결과 및 고찰
  1. 크로마토그램 및 질량스펙트럼
  2. 분석법 검증
  3. 시료의 분석
 결론
 감사의 글
 참고문헌

키워드

Phthalate Plasticizer PVC Analysis GC/MS

저자

  • Na Young Park [ Food Additive Standards Division, Korea Food and Drug Administration, Seoul 122-704, Korea ]
  • Hae Jung Yoon [ Food Chemical Residues Division, National Institute of Food and Drug Safety Evaluation, Seoul 122-704, Korea ]
  • In Shin Kwak [ Food Additives and Packages Division, National Institute of Food and Drug Safety Evaluation, Seoul 122-704, Korea ]
  • Dae Hoon Jeon [ Food Additive Standards Division, Korea Food and Drug Administration, Seoul 122-704, Korea ]
  • Hyun Chul Choi [ Laboratory Audit and Policy Division, Korea Food and Drug Administration, Seoul 122-704, Korea ]
  • Mi Ok Eum [ Food Additive Standards Division, Korea Food and Drug Administration, Seoul 122-704, Korea ]
  • Hyung Il Kim [ Food Additives and Packages Division, National Institute of Food and Drug Safety Evaluation, Seoul 122-704, Korea ]
  • Jun Hyun Sung [ Food Additives and Packages Division, National Institute of Food and Drug Safety Evaluation, Seoul 122-704, Korea ]
  • So Hee Kim [ Food Additives and Packages Division, National Institute of Food and Drug Safety Evaluation, Seoul 122-704, Korea ]
  • Young Ja Lee [ Food Additive Standards Division, Korea Food and Drug Administration, Seoul 122-704, Korea ] Corresponding Author

참고문헌

자료제공 : 네이버학술정보

간행물 정보

발행기관

  • 발행기관명
    한국포장학회 [Korea Society Of Packaging Science & Technology]
  • 설립연도
    1994
  • 분야
    공학>기타공학
  • 소개
    포장기술의 학문적인 발전을 도모하고 국내포장산업의 기술수준 제고를 위하여 선진포장기술 유입의 창구역할을 함

간행물

  • 간행물명
    한국포장학회지 [Journal of Korea Society of Packaging Science & Technology]
  • 간기
    연3회
  • pISSN
    1226-0207
  • 수록기간
    1994~2026
  • 등재여부
    KCI 등재
  • 십진분류
    KDC 530 DDC 620

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