Earticle

점토에 혼입물이 포함되면 수축의 정도를 완화시켜 건조과정에서의 비틀어짐이나 갈라짐을 막아주는 역할을 한다. 이에 삼국시대에 제작된 나주 옹관을 바탕으로 옹관 제조 시 태토에 첨가하는 혼입물의 역할과 환원 소성 시 발생하는 태토의 상태 변화로 인한 옹관의 물성변화를 규명하였다. 나주 오량동 유적의 태토를 이용하여 혼입물 비율(0%, 20%, 40%)을 달리 배합한 재현시료를 제작하고, 여기에 소성온도(1000℃, 1100℃, 1200℃)를 달리하여 소성하였다. 소성 완료된 시료는 육안 관찰, 광학현미경(50배) 관찰, 비중 · 기공률 측정을 통해 물리적 특성을 확인하고, X-선 형광 분석(XRF), X-선 회절 분석(XRD)을 통해 성분의 함량과 특정 광물의 존재 여부를 확인하였다. 그 결과 소성온도 증가에 따른 체적 팽창과 원형의 기공 발생, 혼입물 함량 증가에 따른 비중 증가가 발생하였으며, XRF 분석에서는 SiO2의 증가와 Al2O3의 감소 현상이 일어났다. SiO2의 증가는 혼입물을 이루는 석영 입자의 영향 때문으로 추정되며, 따라서 혼입물의 첨가는 소성온도 증가로 인해 발생되는 태토의 체적 팽창을 억제를 위한 것으로 판단된다.

Adding temper into clay prevents to shrink and crack, or twist the clay during the dry process. The purpose of this study is to identify the role of temper and the physical property of earthenware coffin according to the clay state modification in the reduction firing based on earthenware coffins found in Naju which had been made in Three Kingdom Period. Clay from the Oryang-dong site in Naju was used as circle shaped samples. The samples were tempered with various proportions (0%, 20%, 40%) and fired in various temperature (1000℃, 1100℃, 1200℃). Physical properties were identified by macroscopy, an optical microscope (x50), specific gravity and porosity. Chemical components and existence of specific minerals were identified by analysing XRF and XRD. As a result, the more firing temperature increase, clay volume expansion. To prevent the volume expansion, temper was added.

HPGe 검출기를 이용하여 밀도가 다양한 환경시료에 대한 정밀 분석시 정확한 분석을 위해서는 밀도보정인자가 필요하다. 밀도에 대한 보정인자를 구하기 위해서 본 연구에서는 몬테카를로 코드인 MCNPX 코드를 사용하여 크리스털의 높이, 지름및 코어의 크기와 같은 특성이 다른 세 대의 p-type HPGe 검출기를 모사하고 밀도 1 g/cm3의 교정용 표준시료를 이용하여 모델링을 검증하였다. 검증을 통하여 모델링을 확정한 후 0.3, 0.6, 0.9, 1.0, 1.2, 1.5 g/cm3 밀도를 가진 샘플에 대한 효율을 시뮬레이션하고 밀도보정인자를 도출하였다. 도출된 각 검출기에 대한 밀도보정인자를 비교하였을 때 전 에너지 범위에서 그차이가 거의 없음을 확인하였으며 이는 검출기의 크리스털과 같은 주요 특성에 대해 밀도보정인자가 독립적임을 의미한다.

The precise determination of the activity for each radionuclide in environmental samples requires the self-absorption correction factor. In this research, we derived the self-absorption correction factor for three p-type high purity germanium detectors using the Monte Carlo code MCNPX. These detectors have different characteristics such as crystal diameter, height and size of the core. We compared the calculated full-energy peak efficiency with the experimental value using a standard sample with 1 g/cm3 density and verified the modeling. We simulated the dependency of the full-energy peak efficiency on the 0.3, 0.6, 0.9, 1.0, 1.2 and 1.5 g/cm3 samples and obtained the corresponding self-absorption correction factor. The self-absorption correction factors calculated for the three detectors differ by less than 1% over most of the energy range and sample densities considered. This indicates that the self-absorption correction factors are independent of the crystal characteristics of HPGe detector.

In Korea, most nuclear power plants were designed based on the design response spectrum of Regulatory Guide 1.60 of the NRC. However, in the case of earthquakes occurring in the country, the characteristics of seismic motions in Korea and the design response spectrum differed. The seismic motion in Korea had a higher spectral acceleration in the high-frequency range compared to the design response spectrum. The seismic capacity may be reduced when evaluating the seismic performance of the equipment with high-frequency earthquakes compared with what is evaluated by the design response spectrum for the equipment with a high natural frequency. Therefore, EPRI proposed the inelastic energy absorption factor for the equipment anchorage. In this study, the seismic performance of welding anchorage was evaluated by considering domestic seismic characteristics and EPRI's inelastic energy absorption factor. In order to reflect the characteristics of domestic earthquakes, the uniform hazard response spectrum (UHRS) of Uljin was used. Moreover, the seismic performance of the equipment was evaluated with a design response spectrum of R.G.1.60 and a uniform hazard response spectrum (UHRS) as seismic inputs. As a result, it was confirmed that the seismic performance of the weld anchorage could be increased when the inelastic energy absorption factor is used. Also, a comparative analysis was performed on the seismic capacity of the anchorage of equipment by the welding and the extended bolt.

A risk assessment on the heavy metals including arsenic (As), cupper (Cu), lead (Pb), and zinc (Zn) was investigated by setting exposure routes in agricultural fields. Moreover, the factors requiring improvement in risk assessment were also discussed through a review of the dermal absorption slope factor (SF_abs) and total amount of suspended particles (TSP) in the current risk assessment guidelines. Assessment results show that the total cancer risk (TCR) of As through crop and soil ingestion was 1.51E-03 in adults and 6.37E-4 in children, which indicated a carcinogenic risk (exceeding 1E-05). On the other side, the harzard index (HI) was 3.37 in adults and 1.41 in children, which was evaluated as having a non-carcinogenic risk (>1). The carcinogenic purification targets for As were calculated to be 6.84 mg/kg in adults and 6.86 mg/kg in children, while the non-carcinogenic purification targets were calculated to be 13.43 mg/kg for adults and 22.54 mg/kg for children. When applying SF_abs 61 of the current guidelines, it appears that there is a carcinogenic risk even though the As exposure concentration is below the area of concern 1 standard (25 mg/kg), which suggestes that additional research on this factor is required for the risk assessment. In order to apply the measured suspended particle concentration to risk assessment, TSP should be derived from PM10 using an appropriate correlation equation. As a result, it is suggested to improve the risk assessment guidelines so that the mesured PM10 value measured in the field can be used directly.

용액 순환형 황산망간 용액조 장치를 이용한 중성자 방출류의 절대측정을 위해서 황산망간 용액이 채워진 용액조 안에서 $^{55}$Mn에 의해 흡수되는 중성자 분율에 대한 보정인자를 결정하였다. 이 보정인자, 1/f은 망간, 유황 및 용액에 함유된 불순물 원소들의 원자수 밀도와 유효중성자 포획단면적을 이용하여 결정되었다. 각 원소들의 원자수 밀도의 결정을 위한 용액의 농도는 EDTA 적정에 의한 용량법과 중량법에 의해 분석하였고 불순물 함량은 ICP 방법을 이용하였다. 한편, 유효 중성자 포획 단면적은 자체 작성한 FORTRAN Program EASCAL, Westcotte의 매개변수 및 Axton의 실험식을 사용하여 계산하였다.

The correction factor of neutron fraction absorbed by $^{55}$ Mn in the MnSO$_4$ bath was determined for the absolute measurement of neutron emission rate by using the solution circulation-type manganese sulfate bath system. For the determination of this correction factor, I/f, the atomic number desnsity and the effective neutron capture cross section data of Mn, S and impurity elements in the MnSO$_4$ solution were determined. For the atomic number density determination, the MnSO$_4$ solution concentration was determined by using the volumetric EDTA titration and gravimetric method. The impurity contents were analyzed by using the ICP method. For the calculation of effective neutron capture cross sections, a FORTRAN computer program EASCAL was developed in this study. in which Westcott's parameters and Axton's empirical relations are used.

HPGe 검출기를 이용하여 밀도가 다양한 환경시료에 대한 정밀 분석시 정확한 분석을 위해서는 밀도보정인자가 필요하다. 밀도에 대한 보정인자를 구하기 위해서 본 연구에서는 몬테카를로 코드인 MCNPX 코드를 사용하여 크리스털의 높이, 지름 및 코어의 크기와 같은 특성이 다른 세 대의 p-type HPGe 검출기를 모사하고 밀도 $1g/m^3$의 교정용 표준시료를 이용하여 모델링을 검증하였다. 검증을 통하여 모델링을 확정한 후 0.3, 0.6, 0.9, 1.0, 1.2, $1.5g/m^3$ 밀도를 가진 샘플에 대한 효율을 시뮬레이션하고 밀도보정인자를 도출하였다. 도출된 각 검출기에 대한 밀도보정인자를 비교하였을 때 전 에너지 범위에서 그 차이가 거의 없음을 확인하였으며 이는 검출기의 크리스털과 같은 주요 특성에 대해 밀도보정인자가 독립적임을 의미한다.

The precise determination of the activity for each radionuclide in environmental samples requires the self-absorption correction factor. In this research, we derived the self-absorption correction factor for three p-type high purity germanium detectors using the Monte Carlo code MCNPX. These detectors have different characteristics such as crystal diameter, height and size of the core. We compared the calculated full-energy peak efficiency with the experimental value using a standard sample with $1g/m^3$ density and verified the modeling. We simulated the dependency of the full-energy peak efficiency on the 0.3, 0.6, 0.9, 1.0, 1.2 and $1.5g/m^3$ samples and obtained the corresponding self-absorption correction factor. The self-absorption correction factors calculated for the three detectors differ by less than 1% over most of the energy range and sample densities considered. This indicates that the self-absorption correction factors are independent of the crystal characteristics of HPGe detector.

Using the sbsorption coefficients and the weighting factors of the gray gas, the total emissivities of C $O_{2}$- $H_{2}$O and C $O_{2}$- $H_{2}$O- transient species-soot gas mixtures can be expressed by the following equation, [a numerical formula] Where, $a_{i}$ and $K_{i}$ represent the weighting factor and the absorption coeffient of i-gray gas respectively; L is the pathlength of the gas. This equation is widely used for the analyses of the radiation heat transfer in the combustors of internal combustion engines and in the furnace of external combustion engines. In this work, a simple calculation model of the weighting factor and the absorption coeffient of the above equation was developed. The weighting factors and the absorption coefficients of combustion products were calculated by applying the model to various kinds of fossil fuels such as coal and heavy oil. Then, the computed total emissivities for each fuel and pathlength were compared with measured and calculated values which have been already published in the literatures. The followings were the results obtained through the comparisons between the calculated emissivites and the published values; the developed model for the calculations of the weighting factor and the absorption coefficient of C $O_{2}$- $H_{2}$O and C $O_{2}$- $H_{2}$O- transient species-soot gas mixtures could be applied over the wide ranges of the temperature and the pathlength; the errors between the total emissivities calculted and the values published were maximum 10%, and average 1%, respectively.

연구목적 : 한국판 텔레겐몰입척도(the Korean Version of Tellegen Absorption Scale ; 이하 TAS-K)는 몰입 경험을 표현한 자기-기술식 설문 척도로서 최면감수성을 반영하는 것으로 알려져 있다. 본 연구에서는 TAS-K의 내적 신뢰도를 포함하여 그 요인구조를 알아보고자 하였다. 방법 : 서울 소재 일 대학교의 학생 139명을 대상으로 TAS-K를 사용하여 설문조사를 시행하였다. 척도의 신뢰도 계산을 위해 내적 일관성 지수인 Cronbach's alpha를 산출하였으며 구성 타당도를 검증하기 위해 요인분석을 실시하였다. 결과 : TAS-K의 Cronbach's $\alpha$의 값이 0.82로 나타나 척도의 내적 신뢰도가 비교적 높은 것으로 나타났다. 요인분석을 실시한 결과에서는 고유치 1.0 이상의 요인들을 추출했을 때 3개의 하위요인이 추출되었는데, 1요인은 일시적인 유사 해리 경험, 2요인은 상상적 몰두, 3 요인은 지각적 민감성 등을 각각 반영하고 있었으며, 총 분산의 31.06%를 설명하였다. 결론 : TAS-K는 비교적 내적 신뢰도가 높았으며, 하위요인은 최면감수성과 관련된 특성들을 반영하고 있었다.

Objective : Tellegen Absorption Scale(TAS) is an instrument intended to assess hypnotizability and designed to sample absorbing and self-altering experiences, including dissociative experiences. The present study attempted to identify the internal structure of TAS. Methods : One hundred and thirty nine undergraduates completed the Korean version of Tellegen Absorption Scale(TAS-K). Cronbach's alpha was calculated and factor analyses were done. Results : An exploratory principal-components analysis yielded three factors accounting for 31.06% of variance. Factor 1 included dissociative(dissociation-like) experiences, factor 2 tapped imaginative involvements, and factor 3 had to do with perceptual sensitivity. Conclusion : TAS-K may include absorbing and self-altering experiences.

벼 품종간 Sr-85의 흡수와 작물체 부위별 분포, 그리고 토양으로부터 작물체로 전이되는 Sr-85의 전이계수를 조사하기 위하여 a/2000 pot에 사양토를 공시토양으로 하여 일품벼(만생종)와 오대벼(조생종)를 공시하고 건조토양 1g 당 Sr-85를 각각 무처리, 74Bg과 222Bq를 처리하여 수행한 결과는 다음과 같다. 1 수확기에 일품벼와 오대벼의 Sr-85의 흡수율은 각각 0.39-0.43%, 0.66-0.73%로 오대벼의 흡수율은 전반적으로 일품벼보다 약 1.5배 많았다. 2. 토양으로부터 흡수된 Sr-85의 대부분은 볏짚과 왕겨에 축적되었으며 현미로 전류된 량은 약 1.3%에 불과 하였다. 3. 벼 부위별 Sr-85 농도는 Sr-85 처리량에 따라 높았으며 오대벼는 일품벼보다 모든 부위에서 높은 농도를 보였다. 4. 두 품종에서의 토양-식물체간 전이계수는 품종간 유의성은 없으나 현미 0.037과 볏짚 4.13의 범위였으며 부위별 전이계수는 볏짚>왕겨>현미 순으로 높았다. 5. 토양으로부터 흡수한 Sr-85는 벼의 생장과 수량에는 영향을 미치지 않았다.

To investigate the absorption and transfer factor(TF) of Sr-85 by rice(Oryza sativa L.), experiments were carried out through pot cultivations on a sandy-loam soil treated 74 and 222Bq per gram of soil in a plastic film house. Sr-85 absorption rates of Ilpoombyeo, late maturing variety and Odaebyeo, early maturing variety, at harvesting stage, were 0.39-0.43% and 0.66-0.73%, respectively. Sr-85 absorption rates of Odaebyeo were about 1.5 times higher than those of Ilpoombyeo. Ratios of Sr-85 radiation and Sr-85 concentration in brown rice were much lower compared with those in straw and husk. Sr-85 concentrations in each part of Odaebyeo were remarkably higher than those of Ilpoombyeo. Transfer factor of Sr-85 from soil to plant ranged from 0.037 of brown rice to 4.13 of rice straw at harvesting stage. The order of the Sr-85 transfer factor in plant parts was straw>husk>brown rice. Sr-85 concentrations treated in soil had no effect on the growth and yield of rice.

The modification factor( k-factor) of equivalent damping ratio utilized in the current state-of-the-practice to account for the imperfection of reinforced concrete structures in hysteresis loop is investigated. From this, it is found that the current modification factor does not include the effect of cyclic loading, one of the important characteristic properties of earthquake loading. This could be taken into account by considering the energy absorption efficiency based on the cummulative plastic deformation. From the study, it is suggested that the current approach for the modification factor for the equivalent damping ratio should be reformed.

Near-infrared spectra of methanol-water mixtures and acetonitrile-water mixtures were acquired to find interactions between solvents widely used for reverse-phase liquid chromatography. Mixtures were prepared to give a series of increasing mole fractions of methanol or acetonitrile in water. Data matrices of acquired spectra were analyzed to determine the proper number of principal components of each mixture system using Malinowski's factor indicator function. Initial guess of score matrix and loading matrix were calculated by nonlinear iterative partial least squares (NIPALS) algorithm for faster computation. Iterative target transform factor analysis (ITTFA) was applied to convert the initial estimation of score matrix to true concentration profile and loading matrix to pure spectra of pure components of the mixtures. In case of methanol-water the number of principal components was found to be 4 and those initial guess of factors were converted to the pure spectra of water methanol and two kinds of complexes. In case of acetonitrile-water the number of pure components of the mixtures was found to be 3 and the pure spectrum of acetonitrile-water complex was found. The nonlinear characteristics of concentration profiles of complexes in the solvent mixtures may give a good criteria in understanding their elution characteristics in reverse-phase liquid chromatogrsphy.