Earticle

초록

영어

This study examined the applicability of NMR (Nuclear Magnetic Resonance) spectroscopy for analyzing ignitable liquids— toluene, hexane, and iso-octane—commonly detected at fire scenes, with a focus on time lapse and storage conditions. Experimental results showed that when chloroform (CDCl₃) was used as the solvent, the NMR spectra remained consistent with the reference for up to 30 days, confirming the method's reliability. In contrast, DMSO and methanol did not mix with the samples, rendering analysis infeasible. Furthermore, samples stored in metal cans exhibited abnormal peaks, suggesting contamination, whereas those stored in glass vials retained their spectral integrity. In addition, NMR analysis has the advantage that repeated attempts at sample analysis with non-destructive analysis do not damage the original sample. These findings demonstrate that NMR analysis, when combined with suitable solvents and storage methods, is a reliable tool for preserving and identifying ignitable liquid evidence.

목차

Abstract
1. 서론
1.1 연구배경
1.2 연구목적
2. 이론적 고찰
2.1 가스크로마토그래피(GC, Gas Chromatography)
2.2 핵자기 공명 분광법(NMR, Nuclear Magnetic Resonance)
3. 실험방법
3.1 유류 물질 선정
3.2 NMR 장비
3.3 용매 선택 배경
3.4 시료 준비
4. 실험결과
4.1 톨루엔(Toluene) 분석
4.2 헥세인(Hexane) 분석
4.3 이소옥테인(IsoOctane)분석
4.4 물질별 NMR 분석 결과 종합
4.5 용기 재질에 따른 보관 특성 비교
5. 결론
참고문헌

키워드

저자

• 서형원 [ Hyungwon Seo | 공주소방서 ]
• 조병희 [ Byunghee Cho | 공주소방서 ]
• 허주현 [ Juhyeon Heo | 공주소방서 ]

참고문헌

발행기관

간행물

표지보기 관심저널 등록

• 간행물명

  한국화재감식학회 학회지 [Magazine of Fire Investigation Socity of Korea]

• 간기

  계간

• pISSN

  2092-531X

• 수록기간

  2009~2026

• 등재여부

  KCI 등재

• 십진분류

  KDC 539 DDC 628