The crystallization behavior and microstructural change in glass-ceramics with a cordierite composition were analyzed as a function of concentration and etching time of the HF solution in order to enhance the degree of crystallinity of the glass. Compared to a specimen without etching, the glass frit specimens etched with HF solution showed increased crystalline peak intensities of the μ-cordierite phase in the XRD pattern. The crystal size in the glass matrix also increased with an increasing concentration of the HF solution for the etched glass frit. The crystal peak intensity of the α-cordierite phase in the glass-ceramics made with glass frit etched with 0.5-1.5 wt% HF solution had a slightly higher value than that of pure glass frit regardless of the etching time. The intensity of the specimen with etched glass frit with 3.0 wt% HF solution, however, was lower than that of the specimen of the pure glass frit. Obviously, for the glass-ceramics etched with HF solution of various conditions, the α-cordierite phase is more favorable for crystallization than the α-cordierite phase. This study revealed that the microstructure and ratio of the crystallinity of the α-cordierite phase over the α-cordierite phase in the obtained glass-ceramics could be controlled by changing the HF-etching conditions followed by a heat treatment process.
목차
Abstract 1. Introduction 2. Experimental Procedure 3. Result and Discussion 4. Conclusion References
보안공학연구지원센터(IJHIT) [Science & Engineering Research Support Center, Republic of Korea(IJHIT)]
설립연도
2006
분야
공학>컴퓨터학
소개
1. 보안공학에 대한 각종 조사 및 연구
2. 보안공학에 대한 응용기술 연구 및 발표
3. 보안공학에 관한 각종 학술 발표회 및 전시회 개최
4. 보안공학 기술의 상호 협조 및 정보교환
5. 보안공학에 관한 표준화 사업 및 규격의 제정
6. 보안공학에 관한 산학연 협동의 증진
7. 국제적 학술 교류 및 기술 협력
8. 보안공학에 관한 논문지 발간
9. 기타 본 회 목적 달성에 필요한 사업
간행물
간행물명
International Journal of Hybrid Information Technology
간기
격월간
pISSN
1738-9968
수록기간
2008~2016
십진분류
KDC 505DDC 605
이 권호 내 다른 논문 / International Journal of Hybrid Information Technology Vol.9 No.10