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Determination of Acrylamide in Foods by Solid Phase Microextraction-Gas Chromatography

첫 페이지 보기
  • 발행기관
    한국식품과학회 바로가기
  • 간행물
    Food Science and Biotechnology SCIE KCI 등재 SCOPUS 바로가기
  • 통권
    Volume 18 Number 4 (2009.08)바로가기
  • 페이지
    pp.895-899
  • 저자
    Liangbi Chen, Jinyun Zhao, Haizhu Liu, Xi Chen, Ping Yu
  • 언어
    영어(ENG)
  • URL
    https://www.earticle.net/Article/A110363

※ 원문제공기관과의 협약기간이 종료되어 열람이 제한될 수 있습니다.

원문정보

초록

영어
A new approach for the determination of acrylamide (AM) in foods by solid phase microextraction-gaschromatography (SPME-GC) was established. AM was bromized and transformed to 2-bromoacrylamide (2-BAM). 2-BAMwas then extracted by a commercial SPME fiber, 75-µm Car/PDMS fiber, for GC detection. The influence of extraction anddesorption parameters such as extraction temperature and time, stirring rate, desorption temperature, and time were studiedand optimized. The mass concentration was proportional to the peak area of 2-BPA from 1.0 to 8,000µg/L. The detectionlimit of the SPME-GC for 2-BAM was found to be 0.1µg/L, and the recoveries and relative standard deviations for differentfood samples were 74.5 to 102.0%, and 4.2 to 9.1%, respectively. The presented method was applied to the determination ofAM in fried foods.

목차

Abstract
 Introduction
 Materials and Methods
 Results and Discussion
 References

키워드

solid phase microextraction gas chromatography acrylamide 2-bromoacrylamide food

저자

  • Liangbi Chen [ Department of Chemistry and Environment Engineering, Wuyi University, Fujian 354300, PR China ]
  • Haizhu Liu [ Key Laboratory of Analysis and Detection Technology for Food Safety (Fuzhou University), Ministry of Education,Department of Chemistry, Fuzhou University, Fuzhou 350002, PR China ]
  • Ping Yu [ Key Laboratory of Analysis and Detection Technology for Food Safety (Fuzhou University), Ministry of Education,Department of Chemistry, Fuzhou University, Fuzhou 350002, PR China; Fujian Research Institute of Metric Science, Fuzhou 350003, PR China ]
  • Jinyun Zhao [ Department of Chemistry and Environment Engineering, Wuyi University, Fujian 354300, PR China ]
  • Xi Chen [ Key Laboratory of Analysis and Detection Technology for Food Safety (Fuzhou University), Ministry of Education,Department of Chemistry, Fuzhou University, Fuzhou 350002, PR China ] Corresponding author

참고문헌

자료제공 : 네이버학술정보

간행물 정보

발행기관

  • 발행기관명
    한국식품과학회 [Korean Society of Food Science and Technology]
  • 설립연도
    1970
  • 분야
    농수해양>식품과학
  • 소개
    본회는 사회일반의이익에 공여하기 위하여 공공법인의 운영에 관한 법률의 규정에 따라 식품 과학 전반에 관한 이론 및 기술연구와 그 응용을 촉진 및 보급시키며 학술과 사업을 연계시키고, 나아가 국민의 식생활을 질적, 양적으로 향상시킴을 목적으로 한다.

간행물

  • 간행물명
    Food Science and Biotechnology
  • 간기
    격월간
  • pISSN
    1226-7708
  • 수록기간
    1992~2009
  • 십진분류
    KDC 574 DDC 664

이 권호 내 다른 논문 / Food Science and Biotechnology Volume 18 Number 4

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